| SpectraBase Spectrum ID |
B9wxFsGpOfg |
| Name |
Methapyrilene |
| Source of Sample |
Sigma-Aldrich Company Llc |
| Catalog Number |
Free base of M9125 |
| Lot Number |
Free base of 037F09291V |
| Accessory |
DurasamplIR II |
| CAS Registry Number |
91-80-5 |
| Classification |
antihistamine and anticholinergic |
| Copyright |
Copyright © 2014-2024 John Wiley & Sons, Inc. All Rights Reserved. |
| Formula |
C14H19N3S |
| InChI |
InChI=1S/C14H19N3S/c1-16(2)9-10-17(12-13-6-5-11-18-13)14-7-3-4-8-15-14/h3-8,11H,9-10,12H2,1-2H3 |
| InChIKey |
HNJJXZKZRAWDPF-UHFFFAOYSA-N |
| Instrument Name |
Bio-Rad FTS |
| SMILES |
c1cccnc1N(CCN(C)C)Cc1sccc1 |
| Sample Preparation Procedure |
The HCl salt was dissolved in 0.5 ml water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 ml dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film on the diamond window for ATR-IR. |
| Source of Spectrum |
Forensic Spectral Research |
| Synonyms |
N,N-Dimethyl-N′-(2-pyridinyl)-N′-(2-thienylmethyl)-1,2-ethanediamine |
| Technique |
ATR-Film (MeCl2) (DuraSamplIR II) |
